A practical procedure for carbonyl α-oxidation: synthesis of (2-benzoyloxy)-1,4-cyclohexanedione mono-ethylene ketal

Jones, Teyrnon C. and Tomkinson, Nicholas C. O. (2007) A practical procedure for carbonyl α-oxidation: synthesis of (2-benzoyloxy)-1,4-cyclohexanedione mono-ethylene ketal. Organic Syntheses, 84. pp. 233-241. ISSN 0078-6209

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Abstract

A convenient method for the prepn. of α-acyloxy ketones is described. Oxyacylation of a variety of ketones with O-acyl hydroxyamine derivs. provided the corresponding α-acyloxy ketones in good yields. (2-Benzoyloxy)-1,4-cyclohexanedione mono-ethylene ketal was successfully synthesized from 1,4-cyclohexanedione mono-ethylene ketal.