Kennedy, Alan and Khalaf, Abedawn I. and Suckling, Colin J. and Waigh, Roger D. (2006) 3-Nitro-1-(triisopropylsilyl)-1H-pyrrole. Acta Crystallographica Section E: Structure Reports, 62 (8). o3282-o3284. ISSN 1600-5368
Full text not available in this repository. (Request a copy from the Strathclyde author)Official URL: http://dx.doi.org/10.1107/S1600536806025943
Abstract
The nitration of 1-(triisopropylsilyl)-1H-pyrrole leads to a mixt. of products following partial acid cleavage of the triisopropylsilyl protecting group. Structural detn. showed the isolated products to be 3-nitro-1-(triisopropylsilyl)-1H-pyrrole, C13H24N2O2Si (I), and 2,4-dinitropyrrole. In the solid state, I exists as discrete mols. with only weak C-H...nitro H bonds between them. Crystallog. data are given.
| Item type: | Article |
|---|---|
| ID code: | 34882 |
| Notes: | M1 - Copyright (C) 2011 American Chemical Society (ACS). All Rights Reserved. CAPLUS AN 2006:770761(Journal; Online Computer File) |
| Keywords: | nitration, 4-dinitropyrrole , hydrogen bonds, Chemistry |
| Subjects: | Science > Chemistry |
| Department: | Faculty of Science > Pure and Applied Chemistry |
| Related URLs: | |
| Depositing user: | Pure Administrator |
| Date Deposited: | 21 Oct 2011 13:54 |
| Last modified: | 25 Apr 2012 16:26 |
| URI: | http://strathprints.strath.ac.uk/id/eprint/34882 |
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