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Cytenamide acetic acid solvate

Johnston, Andrea and Florence, A.J. and Fabianni, F.J.A. and Shankland, K. and Bedford, C.T. (2008) Cytenamide acetic acid solvate. Acta Crystallographica Section E: Structure Reports, 64 (6). pp. 1175-1176. ISSN 1600-5368

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Abstract

In the crystal structure of the title compound (systematic name: 5H-dibenzo[a,d]cycloheptatriene-5-carboxamide ethanoic acid solvate), C16H13NO·C2H4O2, the cytenamide and solvent molecules form a hydrogen-bonded R22(8) dimer motif, which is further connected to form a centrosymmetric double ring motif arrangement. The cycloheptene ring adopts a boat conformation and the dihedral angle between the least-squares planes through the two aromatic rings is 54.7 (2)°.